Abstract
This study aimed to characterize nanocellulose extracted from cotton (Gossypium hirsutum) linters. The nanocellulose was subjected to electronic microscopy, thermal analysis, X-ray diffractometry, light scattering, and contact angle. The properties of the nanocellulose are considerably different from the linter. The acidic hydrolyses applied to extract the nanocrystals increased the crystallinity index and the hydrophilicity and decreased the thermal stability. On average, the nanocrystals were 177 nm long and 12 nm wide, with an aspect ratio of 19 when measured by microscopy. The light scattering results were coherent with the crystal dimensions. Cotton linter is a potential source of nanocellulose crystals, particularly to be used in the production of hydrophilic nanocomposites. Extraction of nanocellulose from raw cotton linter does not require pulping
Contents
1. Introduction
2. Materials and methods
2.1. Raw material
2.2. Nanowhiskers preparation
2.3. Chemical characterization
2.4. Electronic microscopy
2.5. Thermal analyses
2.6. FTIR analyses
2.7. X-ray diffractogram
2.8. Contact angle
2.9. Particle size measurement and zeta potential
3. Results and discussion
3.1. Chemical characterization
3.2. Electronic microscopy
3.3. Thermal and FTIR analyses
3.4. X-ray diffractogram
3.5. Contact angle
3.6. Particle size measurement and zeta potential
4. Conclusions